You will be compiling your bibliography and creating an outline of the changes you will make in this sandbox.
Bibliography
As you gather the sources for your Wikipedia contribution, think about the following:
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Bibliography
editEdit this section to compile the bibliography for your Wikipedia assignment. Add the name and/or notes about what each source covers, then use the "Cite" button to generate the citation for that source.
Pagliano, E.; Campanella, B.; D’Ulivo, A.; Mester, Z. Derivatization Chemistries for the Determination of Inorganic Anions and Structurally Related Compounds by Gas Chromatography - A Review. Anal. Chim. Acta 2018, 1025, 12–40. https://doi.org/10.1016/j.aca.2018.03.043.[1]
- Review article that provides and in-depth discussion of the SN2 reaction occuring during silylation. Has additional information on applications.
Myers protective groups – silicon-based protection of the hydroxyl group chem 115. Harvard.edu. https://hwpi.harvard.edu/files/myers/files/7-protective_groups_.pdf (accessed 2024-10-07).
- Shows a large subset of substituents that can be added to silyl groups.
Clayden, J.; Greeves, N.; Warren, S. Organic Chemistry, 2nd ed.; Oxford university press. Oxford, 2012.[2]
- Textbook that includes a surplus of information on substituent reactivity, deprotection, and uses of silylation in enolate trapping.
Parkinson, D. R. (2012-01-01), Pawliszyn, Janusz (ed.), "2.26 - Analytical Derivatization Techniques", Comprehensive Sampling and Sample Preparation, Oxford: Academic Press, pp. 559–595, ISBN 978-0-12-381374-9.[3]
- Describes the use of silylation in gas chromatography.
Ljoncheva, M.; Heath, E.; Heath, D.; Džeroski, S.; Kosjek, T. Contaminants of Emerging Concern: Silylation Procedures, Evaluation of the Stability of Silyl Derivatives and Associated Measurement Uncertainty. Sci. Total Environ. 2023, 899 (165669), 165669. https://doi.org/10.1016/j.scitotenv.2023.165669.[4]
- Discusses silylation thermal stability and electrical voltility.
Examples:
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References
edit- ^ Pagliano, Enea; Campanella, Beatrice; D'Ulivo, Alessandro; Mester, Zoltán (2018-09-26). "Derivatization chemistries for the determination of inorganic anions and structurally related compounds by gas chromatography - A review". Analytica Chimica Acta. 1025: 12–40. doi:10.1016/j.aca.2018.03.043. ISSN 0003-2670.
- ^ Clayden, Jonathan; Greeves, Nick; Warren, Stuart G. (2012). Organic chemistry (2nd ed.). Oxford ; New YorK: Oxford University Press. ISBN 978-0-19-927029-3.
- ^ Parkinson, D. R. (2012-01-01), Pawliszyn, Janusz (ed.), "2.26 - Analytical Derivatization Techniques", Comprehensive Sampling and Sample Preparation, Oxford: Academic Press, pp. 559–595, ISBN 978-0-12-381374-9, retrieved 2024-10-14
- ^ Ljoncheva, M.; Heath, E.; Heath, D.; Džeroski, S.; Kosjek, T. (2023-11-15). "Contaminants of emerging concern: Silylation procedures, evaluation of the stability of silyl derivatives and associated measurement uncertainty". Science of The Total Environment. 899: 165669. doi:10.1016/j.scitotenv.2023.165669. ISSN 0048-9697.
Outline of proposed changes
editClick on the edit button to draft your outline.
Now that you have compiled a bibliography, it's time to plan out how you'll improve your assigned article.
In this section, write up a concise outline of how the sources you've identified will add relevant information to your chosen article. Be sure to discuss what content gap your additions tackle and how these additions will improve the article's quality. Consider other changes you'll make to the article, including possible deletions of irrelevant, outdated, or incorrect information, restructuring of the article to improve its readability or any other change you plan on making. This is your chance to really think about how your proposed additions will improve your chosen article and to vet your sources even further. Note: This is not a draft. This is an outline/plan where you can think about how the sources you've identified will fill in a content gap. |